Past Events

PANalytical Empyrean XRPD Instrument Specific Training- May 8

PANalytical Empyrean
May 8, 2024
1:00PM -2:30PM ET
13-4027 (Campus Map: https://whereis-mit-edu.ezproxyberklee.flo.org/ )

The PANalytical Empyrean diffractometer is an excellent choice for X-ray powder/polycrystalline diffraction measurements with low background. The default mode of this instrument is in Bragg-Brentano parafocusing geometry with CuKa1,Ka2 doublet radiation. Samples can be loaded into a 45-position sample changer to input into the reflection-transmission spinner stage. The instrument has linear position sensitive detector (Pixcel 1D, max count rate: 6.5 x 10^9 cps) which permits rapid data collection up to 255 times faster than with a traditional point detector.

The basic instrument training session will focus on the collection of powder diffraction data using the Bragg Brentano High Definition (BBHD) flat mirror optic, 45-position sample changer, reflection transmission spinner (in reflection geometry) and the Pixcel 1D detector.  This configuration is best suited for high-speed high-resolution data collection from powders and polycrystalline thin films.

Accessories include a Anton Paar CHC+ Cryo-Humidity stage. After you have completed this training, you can request individual training on the humidity stage available with this instrument. 

Users of this instrument should also strongly consider taking a data analysis course to suit their needs, such as the line profile fitting course for crystallite size and microstrain analysis, the Rietveld refinement series for quantitative phase analysis and unit cell analysis, or the Introduction to High Score Plus for qualitative phase identification and database search techniques.

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

Basics of Small Angle X-ray Scattering (SAXS) Lecture- May 8

saxlab
May 8, 2024
10:00AM -11:00AM ET
13-4041 (Campus Map: https://whereis-mit-edu.ezproxyberklee.flo.org/ )

This lecture is intended for people who want to become independent self-user of the small or wide angle X-ray scattering (SAXS) instrument in the MRL X-Ray Lab.  SAXS describes the analysis of any sample that has nanostructured (1-100nm) electron density fluctuations -- i.e., nanoparticles in solution, block co-polymers, ionic liquids, soft matter, etc. Typically nanoscale electron density variations arise as structured (nanoscale object in a lattice), unstructured (in solution), or oriented (fiber or affixed to substrate) therefore treatment of each type of sample is on a case by case basis.  

Students must also attend SAXSLAB instrument specific training course to learn how to put the knowledge obtained in the lecture to practice.

This lecture will survey the fundamentals of small angle X-ray scattering (SAXS), focusing on the bare essentials required to productively collect and analyze SAXS data.  In addition to theory, this lecture will cover practical considerations such as common sources of error and a guide to structural interpretation and justification using SAXS patterns.

Bruker Dektak DXT-A Stylus Profilometer Instrument Training - May 8

dektak
May 8, 2024
10:00AM -12:00PM ET
MIT.nano 13-4139

This group training event will focus on the basic theory and operation of the Bruker Dektak DXT-A Stylus Profilometer 
Users will learn about specifics of the instrument capabilities and strategies for data collection and data quality improvement. Users can bring their own (non-hazardous) samples for this training. We will work together until we are both comfortable with your safe and successful operation of the instrument in a shared facility environment. This is usually one session <2hours. Full independent tool access will be granted upon completion of this training session.
 

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

Bruker Icon XR AFM Basic Training- May 7

May 7, 2024
13:30PM -15:30PM ET
MIT.nano 13-4148

This training event will focus on the basic imaging and operation of the Bruker Icon AFM available at MIT.nano Characterization Facilities. Starting from the basic principles of AFM, users will also learn about cantilever selection and installation, different imaging modes, image quality improvement, and data processing and analysis methods. Users can bring their own samples for this training and SPM probes are provided. Notice, users must supply their own probes for followup qualification sessions. Full independent tool access will be granted upon completion of 2 additional one-on-one supervised use sessions that will be coordinated with the staff member during this small group training.

The Icon XR has many SPM modes including contact and PeakForce tapping mode with ScanAsyst, Magnetic Force Microscopy, Piezo Force Microscopy, conducting atomic force microscopy (AFM). There are also additional features such as electrical characterization from 80 fA to 1 uA with 10 nm spatial resolution, Kelvin Force Probe Microscopy with amplitude or frequency feedback, and pixel-by-pixel quantitative force characterization to probe material properties. Following the basic training session, users can coordinate an advanced mode specific training with the MIT.nano staff.

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

FAB.nano Wet Chemical Process Training - May 7

May 7, 2024
1-2:30pm
MIT.nano (12-4001)

The Wet Chemical Process Training provides an introduction for all work with liquid chemicals in Fab.nano. Completion is required for any use of fume hoods or wet benches (including solvents, hands-on training for spin coaters, corrosive hoods and wet benches).

The training is also a prerequisite for 24-hour access to the Fab.nano facility, as it provides the relevant safety foundations.

Laue Instrument Specific Training- May 7

Laue
May 7, 2024
1:00PM - 3:00PM ET
13-4027 (Campus Map: https://whereis-mit-edu.ezproxyberklee.flo.org/ )

This instrument training will teach users how to use the Multiwire Back-Reflection Laue Diffractometer to determine the orientation of single crystals and to determine if single crystals are possibly twinned.

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

Fourier Transform Infrared (FTIR) Spectrometer Instrument Training - May 7

FTIR
May 7, 2024
1:00PM -3:00PM ET
MIT.nano 13-4139

This group training event will focus on the basic theory and operation of the Fourier Transform Infrared Spectrometer 
Users will learn about specifics of the instrument configurations, available accessories and strategies for data collection and data quality improvement. Users can bring their own (non-hazardous) samples for this training in whatever form is convenient. We will work together until we are both comfortable with your safe and successful operation of the instrument in a shared facility environment. This is usually one session <2hours. Full independent tool access will be granted upon completion of this training session.
 

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

XRF Instrument and Data Analysis Training- May 7

Bruker XRF handheld
May 7, 2024
10:00AM - 11:00AM ET
13-4027 (Campus Map: https://whereis-mit-edu.ezproxyberklee.flo.org/ )

This course will consist of a lecture teaching the basic principals of XRF analysis and hands-on training how to use the handheld XRF spectrometer and data analysis software to determine the elemental composition of samples.

Active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event. 

PHI Versaprobe II XPS training - May 7

PHI XPS
May 7, 2024
9:45AM-5:00PM
Presentation on Zoom and Hands on in 13-4137
The introductory group class follows this schedule:
        9:45 - 11:30        Interactive Zoom presentation (link
        Noon to 1:00      XPS lab:  Introduction to the instrument, sample mounting, initial software set-up
        1:00 - 2:00          Break 
        2:00 - 5:00          XPS lab: analyses of trainees’ samples
 
During the lab sessions,

      •  Trainees receive a tour of PHI Versaprobe II instrument components and vacuum system design
      •  Record-keeping, sample mounting, instrument set-up and sample pumpdown are demonstrated
      •  In-lab and online resources for data analysis are introduced
      •  Data collection and analysis are demonstrated using the trainees' samples
 

The introductory group class is followed during the week by individual trainee hands-on analysis sessions, continuing analysis of the trainee’s samples. Time is pre-reserved for this purpose and is available on a first-come, first-served basis.  


With careful attention to instrument operation protocol, most users feel ready to take their “driver’s test” for self-user XPS access during their second or third hands-on session. 

The driver’s test consists of a hands-on analysis session just like the user’s previous analysis sessions -- but with each step in the operating procedure the user describes what they’re doing, and why they’re doing it, before they do it.  The user is also quizzed to confirm good understanding of the vacuum system. 

FAB.nano New User Quick-Start - May 7

May 7, 2024
9am-noon
Fab.nano Cleanroom (12-3101)

All users without previous cleanroom work experience are required to take the quick-start training. Waivers for prior experience will be handled during the Fab.nano orientation.

The quick-start provides hands-on training to new users, by following through a simple 1-mask process in a small group. You will gain familiarity with entering the lab, handling samples, learn about deposition, lithography and etch tools, and how to verify process results.

An active MIT.nano user account is required to participate in this training. Please setup an account prior to registering for the training event.

Because we are working in the lab, please wear long pants and full shoes

Please have the Fab.nano Orientation completed before the quick-start event.